3-Iodo-4-methylbenzyl alcohol → 3-Iodo-4-methylbenzaldehyde
Reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[CH3:10])[CH2:5][OH:6]>C(Cl)Cl.O=[Mn]=O>[I:1][C:2]1[CH:3]=[C:4]([CH:7]=[CH:8][C:9]=1[CH3:10])[CH:5]=[O:6]Participants
4
Reactant 1
Product 1
Reagents, catalysts & solvents 2
Procedure
A mixture of 1.0 mmol of this alcohol and 5.0 mmol of MnO2 in 5 mL of CH2Cl2 was stirred for 16 h at rt. Chromatography provided 3-iodo-4-methylbenzaldehyde.
Sources & evidence
- ORD record
- ord-bd82a5043a4441d6bb653b1731c79827
- Source dataset
- uspto-grants-1998_03
- Patent number
- US05731432
Reaction notes
Loading…