m-Anisoyl chloride → 5-Methoxy-2-(3-methoxybenzoyl)benzoic acid

HRID 29937

Reaction equation

HRID 29937 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6](Cl)=[O:7].Br[C:13]1[CH:21]=[CH:20][C:19]([O:22][CH3:23])=[CH:18][C:14]=1[C:15]([OH:17])=[O:16]>>[CH3:23][O:22][C:19]1[CH:20]=[CH:21][C:13]([C:6](=[O:7])[C:5]2[CH:9]=[CH:10][CH:11]=[C:3]([O:2][CH3:1])[CH:4]=2)=[C:14]([CH:18]=1)[C:15]([OH:17])=[O:16]

Participants

3

Reactant 2

HCID 74374m-Anisoyl chlorideHCID 899062-Bromo-5-methoxybenzoic acid

Product 1

HCID 3340815-Methoxy-2-(3-methoxybenzoyl)benzoic acid

Procedure

This compound is obtained according to the procedure described in 1.1. by reacting 3-methoxybenzoyl chloride and 2-bromo-5-methoxybenzoic acid after halogen-lithium exchange. It is used in crude form in the following reaction.

Workup

  1. customThis compound is obtained
  2. customin the following reaction

Sources & evidence

ORD record
ord-fec9b8467d99458ebf8221c1099c5cf9
Source dataset
uspto-grants-2008_09
Patent number
US07423030B2

Linked notes

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