Cyanocyclobutane → HCID 59792382, compound

HRID 31652Notes

Reaction equation

[CH:1]1([C:4]23[O:11][CH2:10][C:7]([CH2:12][OH:13])([CH2:8][O:9]2)[CH2:6][O:5]3)[CH2:3][CH2:2]1.[CH:14]1(C#N)CCC1>>[CH:1]1([C:4]23[O:5][CH2:6][C:7]([CH2:12][OH:13])([CH2:8][O:9]2)[CH2:10][O:11]3)[CH2:3][CH2:2][CH2:14]1

Participants

Reactant 2

HCID 78148Cyanocyclobutane

HCID 59792605HCID 59792605, compound

Product 1

HCID 59792382HCID 59792382, compoundYield 51%

Procedure

The same procedure as in the steps (37a) to (37c) of Example 37 was repeated using cyclobutanecarbonitrile to obtain the title compound (15 g, total yield: 51%) as a light yellow oil.

Sources & evidence

ORD record: ord-8161260e18284c7b83865735b591d5c1
Source dataset: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07425634B2

Reaction notes

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