HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → 2,3-Dichloro-6-iodobenzoic acid chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 2,3-Dichloro-6-iodobenzoic acid | HCID 22008816 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 2,3-Dichloro-6-iodobenzoic acid chloride | HCID 54292031 | — |
Reaction Steps
DMF (one drop) was added to a stirred solution of 2,3-dichloro-6-iodobenzoic acid (1.53 g, 4.83 mmol) and oxalyl chloride (2 ml) in ethyl acetate (20 ml). After 2 hours, the solution was evaporated and the product was used immediately.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06211189B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-7726a461dd284d93b0a1fcdd654e9b25 |
| Source note | uspto-grants-2001_04 |