Formic Acid → 1-Cyano-1-formylaminocyclopentane

HRID 322811

Reaction equation

HRID 322811 reaction equation
[NH2:1][C:2]1([C:7]#[N:8])[CH2:6][CH2:5][CH2:4][CH2:3]1.[CH:9](O)=[O:10]>O>[C:7]([C:2]1([NH:1][CH:9]=[O:10])[CH2:6][CH2:5][CH2:4][CH2:3]1)#[N:8]

Participants

4

Reactant 2

HCID 284Formic AcidHCID 21068971-Aminocyclopentanecarbonitrile

Product 1

HCID 212029501-Cyano-1-formylaminocyclopentane

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

11.0 g (0.1 mol) of 1-amino-1-cyanocyclopentane and 10 ml of 85% formic acid were placed in an apparatus equipped with water-separatory distillation head and boiled for 3 hours. The reaction mixture was then evaporated to constant weight in vacuo.

Workup

  1. customThe reaction mixture was then evaporated to constant weight in vacuo

Sources & evidence

ORD record
ord-def3b84f363245bdb19ba349862925db
Source dataset
uspto-grants-2001_04
Patent number
US06211382B1

Linked notes

Loading…