3-Iodobenzoic acid → 3-Iodobenzoyl chloride

HRID 322963

Reaction equation

HRID 322963 reaction equation
[I:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5](O)=[O:6].S(Cl)([Cl:13])=O>>[I:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([Cl:13])=[O:6]

Participants

3

Reactant 2

HCID 120603-Iodobenzoic acidHCID 24386Thionyl Chloride

Product 1

HCID 743783-Iodobenzoyl chloride

Procedure

A stirred suspension of 3-iodobenzoic acid (8.84 g) in thionyl chloride (44 mL) is heated at reflux for 30 minutes. The dark brown solution is evaporated to give 3-iodobenzoyl chloride (9.8 g) as a brown oil.

Workup

  1. temperatureis heated
  2. temperatureat reflux for 30 minutes
  3. customThe dark brown solution is evaporated

Sources & evidence

ORD record
ord-b827ff56829d41e09cc67ff193ea896a
Source dataset
uspto-grants-2001_04
Patent number
US06211234B1

Linked notes

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