HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → 2,6,7-Trichloro-3-iodoimidazo[1,2-A]pyridine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | 2,6,7-TRICHLOROIMIDAZO[1,2-A]PYRIDINE | HCID 10680521 | — |
| Reactant | 2,6-Dichloro-3-iodoimidazo[1,2-a]pyridine | HCID 11141504 | — |
| Product | 2,6,7-Trichloro-3-iodoimidazo[1,2-A]pyridine | HCID 10871733 | 82% |
Reaction Steps
Following the preparation of compound 19, compound 16 (1.7 g, 7.7 mmol) was treated with NIS to give 2.2 g (82%) of compound 25 as a white crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06214801B1 |
| Source dataset | uspto-grants-2001_04 |
| ORD ID | ord-7b9cf3b95c324769abf4f727face5d90 |
| Source note | uspto-grants-2001_04 |