Ethyl Methacrylate → Ethyl Methacrylate Ethylene Glycol Dimethacrylate
Reaction equation
CCCCCCCCCCCCOS([O-])(=O)=O.[Na+].S(OOS([O-])(=O)=O)([O-])(=O)=O.[Na+].[Na+].[C:31]([O:36][CH2:37][CH3:38])(=[O:35])[C:32]([CH3:34])=[CH2:33].[C:39]([O:44][CH2:45][CH2:46][O:47][C:48](=[O:52])[C:49]([CH3:51])=[CH2:50])(=[O:43])[C:40]([CH3:42])=[CH2:41]>>[C:31]([O:36][CH2:37][CH3:38])(=[O:35])[C:32]([CH3:34])=[CH2:33].[C:39]([O:44][CH2:45][CH2:46][O:47][C:48](=[O:52])[C:49]([CH3:51])=[CH2:50])(=[O:43])[C:40]([CH3:42])=[CH2:41]Participants
5
Procedure
Same as C5 except that monomer emulsion was composed of 5 g of SDS, 1 g of sodium persulfate, 180 g of ethyl methacrylate, and 20 g of ethylene glycol dimethacrylate. Tg was 74° C., average particle size was 33 nm and % solids was 20.4%.