3'-Aminoacetophenone → HCID 178507142, compound

Reaction equation

[NH2:1][C:2]1[N:7]([C:8]2[CH:13]=[CH:12][C:11](N)=[CH:10][CH:9]=2)[CH2:6][N:5]=[C:4]2[O:15][CH:16]=[CH:17][C:3]=12.CC(C1C=CC=C([NH2:27])C=1)=O>>[NH2:1][C:2]1[N:7]([C:8]2[CH:13]=[CH:12][CH:11]=[C:10]([NH2:27])[CH:9]=2)[CH2:6][N:5]=[C:4]2[O:15][CH:16]=[CH:17][C:3]=12

Participants

Reactant 2

HCID 74173'-Aminoacetophenone

HCID 178507147HCID 178507147, compound

Product 1

HCID 178507142HCID 178507142, compound

Procedure

The compound was prepared following the procedures described in making 4-Amino-3-(4-aminophenyl)furo[2,3-d]pyrimidine (9), using 3-aminoacetophenone instead of 4-aminoacetophenone as starting material. MS(ES) m/e 227 [M+H]+.

Workup

customThe compound was prepared

Sources & evidence

ORD record: ord-fc6d186a3eb24047b0b5a5d5b53d5436
Source dataset: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07427623B2

Reaction notes

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