1,5-Dibromopentane → HCID 54161839, compound

Reaction equation

[CH3:1][O:2][C:3](=[O:14])[CH2:4][CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[OH:13].[Br:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20]Br>>[CH3:1][O:2][C:3](=[O:14])[CH2:4][CH2:5][CH2:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][Br:15]

Participants

Reactant 2

HCID 81001,5-Dibromopentane

HCID 12079672Benzenebutanoic acid, 2-hydroxy-, methyl ester

Product 1

HCID 54161839HCID 54161839, compoundYield 81%

Procedure

Using the procedure of example 108, 2-hydroxybenzenebutanoic acid methyl ester was converted into the title compound by alkylation with 1,5-dibromopentane, in 81% yield, as a colorless oil.

Sources & evidence

ORD record: ord-eed285e8a69042c8910d19186c8c8d39
Source dataset: uspto-grants-1993_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05273999

Reaction notes

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