Pivaloyl chloride → HCID 86734639, compound
Reaction equation
[CH3:1][N:2]([CH2:22][CH2:23][OH:24])[C:3](=[O:21])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10]/[CH:11]=[CH:12]\[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20].[CH3:25][C:26]([CH3:31])([CH3:30])[C:27](Cl)=[O:28]>>[CH3:1][N:2]([CH2:22][CH2:23][O:24][C:27](=[O:28])[C:26]([CH3:31])([CH3:30])[CH3:25])[C:3](=[O:21])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10]/[CH:11]=[CH:12]\[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH3:20]Participants
3
Procedure
N-methyl-N-(2-trimethylacetoxyethyl)oleamide was prepared by the procedure of example 1 from 34 gms. (0.1 mole) of N-methyl-N-(2-hydroxyethyl)oleamide and 12 gms. (0.1 mole) trimethylacetyl chloride. The structure of the final product was characterized on the basis of IR and NMR spectral analyses as described in example 1.
Workup
- customN-methyl-N-(2-trimethylacetoxyethyl)oleamide was prepared by the procedure of example 1 from 34 gms
Sources & evidence
- ORD record
- ord-b6528995cbc64fb4ab717a91a2725787