Phenol → HCID 57485333, compound

Reaction equation

[C:1]1([OH:7])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[CH3:8][CH:9]([CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:10](Cl)=[O:11]>>[CH3:8][CH:9]([CH2:13][C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1)[C:10]([O:7][C:1]1[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1)=[O:11]

Participants

Reactant 2

HCID 996Phenol

HCID 11679924alpha-Methylbenzenepropanoyl chloride

Product 1

HCID 57485333HCID 57485333, compound

Procedure

The procedure as described in Example 4a) was repeated with phenol (30.5 mmol) and 2-methyl-3-phenylpropanoyl chloride (30.5 mmol). The crude product (5.51 g, 75%) was used without further purification in the next step.

Workup

customThe crude product (5.51 g, 75%) was used without further purification in the next step

Sources & evidence

ORD record: ord-e1ffee135ef84de49a20f8808905726e
Source dataset: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08877704B2

Reaction notes

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