2-Fluoro-4-iodoaniline → HCID 57773671, compound

HRID 333117

Reaction equation

[N:1]([C:4]1[CH:9]=[CH:8][C:7]([S:10]([NH2:13])(=[O:12])=[O:11])=[CH:6][CH:5]=1)=[C:2]=[S:3].[F:14][C:15]1[CH:21]=[C:20]([I:22])[CH:19]=[CH:18][C:16]=1[NH2:17]>>[F:14][C:15]1[CH:21]=[C:20]([I:22])[CH:19]=[CH:18][C:16]=1[NH:17][C:2](=[S:3])[NH:1][C:4]1[CH:5]=[CH:6][C:7]([S:10]([NH2:13])(=[O:11])=[O:12])=[CH:8][CH:9]=1

Participants

Reactant 2

HCID 1856942-Fluoro-4-iodoaniline

HCID 5213594-Isothiocyanatobenzenesulfonamide

Product 1

HCID 57773671HCID 57773671, compound

Procedure

The subject compound was prepared utilizing the procedure described above from 4-isothiocyanatobenzenesulfonamide and 2-fluoro-4-iodoaniline. 1H NMR (400 MHz, DMSO-d6) δ 10.35 (s, 1H), 9.77 (s, 1H), 7.86-7.37 (m, 7H), 7.29 (bs, 2H); (M+H)+ (452).

Workup

customThe subject compound was prepared

Sources & evidence

ORD record: ord-3f8eccc241d44cfb8dc30c26caeee8c7
Source dataset: uspto-grants-2014_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08877970B2

Linked notes

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