1(2H)-Phthalazinone → HCID 66598667, compound

HRID 334802

Reaction equation

HRID 334802 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][C:6]#[C:7][C:8]1[CH:13]=[CH:12][CH:11]=[CH:10][N:9]=1.[C:14]1(=[O:24])[C:23]2[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=2)[CH:17]=[N:16][NH:15]1>>[N:9]1[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=1[C:7]#[C:6][CH2:5][CH2:4][CH2:3][CH2:2][N:15]1[N:16]=[CH:17][C:18]2[C:23](=[CH:22][CH:21]=[CH:20][CH:19]=2)[C:14]1=[O:24]

Participants

3

Reactant 2

HCID 83941(2H)-PhthalazinoneHCID 20331212HCID 20331212, compound

Product 1

HCID 66598667HCID 66598667, compound

Procedure

The title compound was prepared in accordance with the general method of Example 242(B), from 2-(6-bromohex-1-ynyl)pyridine (138 mg, 0.578 mmol) and phthalazin-1(2H)-one (80 mg, 0.55 mmol).

Sources & evidence

ORD record
ord-2861f9b58cb94de496a8a1129935cd19
Source dataset
uspto-grants-2014_11
Patent number
US08883826B2

Linked notes

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