4-Heptanamine → 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide

Participants

Role	Name	HCID	Charge
Reactant	4-Heptanamine	HCID 38665	—
Reactant	3-Amino-4-hydroxybenzoic acid	HCID 65083	—
Product	3-amino-4-hydroxy-N-(1-propylbutyl)benzamide	HCID 66773120	57%

Reaction Steps

3-amino-4-hydroxy-N-(1-propylbutyl)benzamide was prepared in a similar manner to example 4 using 3-Amino-4-hydroxybenzoic acid and 4-heptylamine. Yield 57%. 1H NMR (500 MHz, CDCl3): δ 0.93 (t, 6H); 1.26-1.51 (m, 8H); 4.09 (m, 1H); 6.74 (m, 1H); 7.05 (s, 1H); 7.43 (m, 2H); 7.77 (m, 2H). MS: (251, M+H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08895050B2
Source dataset	uspto-grants-2014_11
ORD ID	ord-2e3ce0e3ec9140c6a2db21225c34d2f5
Source note	uspto-grants-2014_11