HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetramethyl orthocarbonate → 2-Methoxy-benzooxazole-5-carboxylic Acid (1-propyl-butyl)-amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetramethyl orthocarbonate | HCID 74613 | — |
| Reactant | 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide | HCID 66773120 | — |
| Product | 2-Methoxy-benzooxazole-5-carboxylic Acid (1-propyl-butyl)-amide | HCID 57527989 | 60% |
Reaction Steps
Prepared in a similar manner to example 41 using 3-amino-4-hydroxy-N-(1-propylbutyl)benzamide (example 41a) and tetramethylorthocarbonate. Yield: 60%. mp 137-138° C.; MS (M+H, 291.10).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08895050B2 |
| Source dataset | uspto-grants-2014_11 |
| ORD ID | ord-9e42a0aa231c471187e6b56d3954802d |
| Source note | uspto-grants-2014_11 |