Glycine → Trehalose glycine

HRID 339479

Reaction equation

HRID 339479 reaction equation
[CH2:1]([OH:23])[C@H:2]1[O:7][C@H:6]([O:8][C@H:9]2[O:14][C@H:13]([CH2:15][OH:16])[C@@H:12]([OH:17])[C@H:11]([OH:18])[C@H:10]2[OH:19])[C@H:5]([OH:20])[C@@H:4]([OH:21])[C@@H:3]1[OH:22].O.O.[NH2:26][CH2:27][C:28]([OH:30])=[O:29]>O>[CH2:15]([OH:16])[C@H:13]1[O:14][C@H:9]([O:8][C@H:6]2[O:7][C@H:2]([CH2:1][OH:23])[C@@H:3]([OH:22])[C@H:4]([OH:21])[C@H:5]2[OH:20])[C@H:10]([OH:19])[C@@H:11]([OH:18])[C@@H:12]1[OH:17].[NH2:26][CH2:27][C:28]([OH:30])=[O:29]

Participants

5

Reactant 3

HCID 750GlycineHCID 181978Trehalose, dihydrateHCID 178435178HCID 178435178, compound

Product 1

HCID 69122788Trehalose glycine

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

Workup

  1. additionwas added at room temperature
  2. customwas obtained
  3. additionWithout adding any acid

Sources & evidence

ORD record
ord-e6a98632f7324014862b2951e80639e0
Source dataset
uspto-grants-2014_11
Patent number
US08895506B2

Linked notes

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