2-(Methylamino)ethanol → N-Methyl-N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethanolamin

HRID 34564

Reaction equation

HRID 34564 reaction equation
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[CH3:23][NH:24][CH2:25][CH2:26][OH:27]>>[CH3:23][N:24]([C:4](=[O:6])[CH:3]=[C:2]([CH3:1])[CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])[CH2:25][CH2:26][OH:27]

Participants

3

Reactant 2

HCID 80162-(Methylamino)ethanolHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

Product 1

HCID 54048398N-Methyl-N-(3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoyl)-ethanolaminYield 92%

Procedure

The procedure of Example 1 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 2.4 ml of N-methylethanolamine were used. 6.6 g (yield 92%) of the title compound was obtained as a colorless oil.

Sources & evidence

ORD record
ord-d5106581954f4fe4a6f2c2f345dfca3c
Source dataset
uspto-grants-1988_08
Patent number
US04762829

Linked notes

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