2-Aminomethyl-1-ethylpyrrolidine → 2-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoylaminomethyl)-1-ethylpyrrolidine

HRID 34569

Reaction equation

HRID 34569 reaction equation
[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([OH:6])=O.[NH2:23][CH2:24][CH:25]1[CH2:29][CH2:28][CH2:27][N:26]1[CH2:30][CH3:31]>>[CH3:1][C:2]([CH2:7][CH2:8][CH:9]=[C:10]([CH3:22])[CH2:11][CH2:12][CH:13]=[C:14]([CH3:21])[CH2:15][CH2:16][CH:17]=[C:18]([CH3:20])[CH3:19])=[CH:3][C:4]([NH:23][CH2:24][CH:25]1[CH2:29][CH2:28][CH2:27][N:26]1[CH2:30][CH3:31])=[O:6]

Participants

3

Reactant 2

HCID 1172952-Aminomethyl-1-ethylpyrrolidineHCID 1285703,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenic acid

Product 1

HCID 545414572-(3,7,11,15-Tetramethyl-2,6,10,14-hexadecatetraenoylaminomethyl)-1-ethylpyrrolidineYield 94%

Procedure

The procedure of Example 9 was repeated except that 6.1 g of 3,7,11,15-tetramethyl-2,6,10,14-hexadecatetraenoic acid and 3.8 g of 2-aminomethyl-1-ethylpyrrolidine were used as starting materials. 7.8 g (yield 94%) of the title compound was obtained as a brown oil.

Sources & evidence

ORD record
ord-dda9c99e1c1445d2964589abf8008a1d
Source dataset
uspto-grants-1988_08
Patent number
US04762829

Linked notes

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