HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Phenoxybenzaldehyde → 5,5-Dimethyl-2-(3-phenoxyphenyl)-3-(4-phenylbutyl)-4-thiazolidinone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Phenoxybenzaldehyde | HCID 38284 | — |
| Reactant | 2-Mercapto-2-methylpropanoic acid | HCID 78421 | — |
| Reactant | Benzenebutanamine | HCID 83242 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5,5-Dimethyl-2-(3-phenoxyphenyl)-3-(4-phenylbutyl)-4-thiazolidinone | HCID 19990602 | — |
Reaction Steps
Using the procedures of Example 5, the title compound was prepared as a light yellow viscous oil (8.4 g, 65%) from 5.9 g (0.030 mole) of 3-phenoxybenzaldehyde (Fluka), 3.6 g (0.030 mole) of 2-mercapto-2-methylpropionic acid, and 4.6 g (0.030 mole) of 4-phenylbutylamine after refluxing in 250 ml of benzene overnight.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05061720 |
| Source dataset | uspto-grants-1991_10 |
| ORD ID | ord-79c0bbcc9ca8426eb94a9eff610b6370 |
| Source note | uspto-grants-1991_10 |