1,3-Butanediol → Diisocyanate Diurethane

HRID 34683

Reaction equation

HRID 34683 reaction equation
CC1C(=CC(=CC=1)N=C=O)[N:4]=[C:5]=[O:6].C(O)C[CH:16]([OH:18])[CH3:17]>>[N-:4]=[C:5]=[O:6].[N-:4]=[C:5]=[O:6].[NH2:4][C:5]([O:18][CH2:16][CH3:17])=[O:6].[NH2:4][C:5]([O:18][CH2:16][CH3:17])=[O:6]

Participants

3

Procedure

About 348 parts of toluene diisocyanate are mixed with 90 parts of 1,3-butylene glycol and reacted at 30° C. to form a diurethane diisocyanate. About 260 parts of hydroxyethyl methacrylate are added to the resultant diurethane diisocyanate and the mixture heated at 50° C. until the --NCO content is zero.

Workup

  1. customreacted at 30° C.

Sources & evidence

ORD record
ord-4ac42ee506ea4e9983a87d419018aa3c
Source dataset
uspto-grants-1988_08
Patent number
US04762887

Linked notes

Loading…