Dimethyl N-cyanodithioiminocarbonate → HCID 178503921, compound

HRID 35046

Reaction equation

HRID 35046 reaction equation
N1(CC2C=C(C=CC=2)OCCCN)CCCCC1.C(N=C(SC)SC)#N.[CH3:27][S:28][C:29](=[N:48][C:49]#[N:50])[NH:30][CH2:31][CH2:32][CH2:33][O:34][C:35]1[CH:40]=[CH:39][CH:38]=[C:37]([CH2:41][N:42]2[CH2:47]CCC[CH2:43]2)[CH:36]=1>>[C:49]([N:48]=[C:29]([S:28][CH3:27])[NH:30][CH2:31][CH2:32][CH2:33][O:34][C:35]1[CH:40]=[CH:39][CH:38]=[C:37]([CH2:41][N:42]([CH3:47])[CH3:43])[CH:36]=1)#[N:50]

Participants

4

Reactant 3

HCID 66289Dimethyl N-cyanodithioiminocarbonateHCID 102205613-(3-(Piperidin-1-ylmethyl)phenoxy)propan-1-amineHCID 178503920HCID 178503920, compound

Product 1

HCID 178503921HCID 178503921, compound

Procedure

Similarly prepared from 3-[3-(1-piperidinylmethyl)phenoxy]propanamine] (10 g) and cyanocarbonimidodithioic acid, dimethyl ester (5.84 g) was N'-cyano-N-[3-[3-(1-piperidinylmethyl)phenoxy]propyl]carbamimidothioic acid methyl ester (11.5 g) m.p. 89°-90°.

Sources & evidence

ORD record
ord-93a4e52233074ff39d7d35ab7382ad49
Source dataset
uspto-grants-1988_08
Patent number
US04764612

Linked notes

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