Reaction equation
[O-:1][Si:2]([O-:4])=[O:3].[Na+:5].[Na+].[OH-:7].[Na+]>>[Si:2]([O-:7])([O-:4])([O-:1])[O-:3].[Na+:5].[Na+:5].[Na+:5].[Na+:5]Participants
3
Procedure
(Comparison) 1600 kg of water glass with an SiO2/Na2O ratio of 2.06 and an active substance content of 45.5% were admixed with 36.8 kg of sodium hydroxide solution (48% strength) and spray-dried in a spray tower from Kestner to give an amorphous sodium silicate having an active substance content of 83%. 15 kg of the amorphous sodium silicate are heat-treated at 720° C. for 90 min in a muffle furnace (Nabertherm, model W1000/H). A second batch is treated identically. The chilled materials (about 24 kg) are pulverized using a jaw crusher and a disk mill.
Workup
- customspray-dried in a spray tower from Kestner
Sources & evidence
- ORD record
- ord-ee6f125aac904e21a82a287e76f823af
- Source dataset
- uspto-grants-2004_06
- Patent number
- US06743766B1
Linked notes
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