HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dichlorobenzene → 3,4'-Dichlorodiphenyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dichlorobenzene | HCID 4685 | — |
| Reactant | 3-Chlorophenol | HCID 7933 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Dimethylacetamide | HCID 31374 | — |
| Product | 3,4'-Dichlorodiphenyl ether | HCID 81283 | — |
Reaction Steps
80 g (1 mol) of 50% sodium hydroxide are added to a solution of 128.1 g (1 mol) of 3-chlorophenol in 1325 g (9 mol) of 1,4-dichlorobenzene and 27 g (0.3 mol) of dimethylacetamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04766253 |
| Source dataset | uspto-grants-1988_08 |
| ORD ID | ord-dca331bd7c724979a783dd4f38301cb2 |
| Source note | uspto-grants-1988_08 |