HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichlorodiphenylsilane → Diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichlorodiphenylsilane | HCID 6627 | — |
| Reactant | Methyl 3,5,6-trichloro-2-pyridyl carbonate | HCID 20218094 | — |
| Catalyst | Tetrabutylammonium Chloride | HCID 70681 | — |
| Product | Diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane | HCID 20508437 | — |
Reaction Steps
In the manner described in Examples 1-7, diphenyldichlorosilane was reacted with about two moles of methyl 3,5,6-trichloro-2-pyridyl carbonate in the presence of tetrabutylammonium chloride to produce a good yield of diphenyl bis(3,5,6-trichloro-2-pyridyloxy)silane, a crystalline solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04375549 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-33bc60857ac645f1a3e3a467526a3167 |
| Source note | uspto-grants-1983_03 |