Salicylic Acid → 5-(2-Propylpentanoyl)Salicylic Acid

Participants

Role	Name	HCID	Charge
Reactant	Salicylic Acid	HCID 338	—
Reactant	2-Propylvaleryl chloride	HCID 76240	—
Product	5-(2-Propylpentanoyl)Salicylic Acid	HCID 13748710	52%

Reaction Steps

This compound is prepared by a Friedel-Crafts reaction from salicylic acid and 2-propylpentanoyl chloride. The acid yield is 52%. The recrystallization is done in petroleum ether. The melting point is 118° C.

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US04767750
Source dataset	uspto-grants-1988_08
ORD ID	ord-6261f72d624144a1932153c5569dbb6b
Source note	uspto-grants-1988_08