HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloro-4-(chlorosulfonyl)benzoic acid → rel-2-Chloro-5-(((3R,5S)-3,5-dimethyl-1-piperidinyl)sulfonyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloro-4-(chlorosulfonyl)benzoic acid | HCID 188427 | — |
| Reactant | 2-Chloro-4-(cis-3,5-dimethylpiperidinosulfonyl)benzoic acid | HCID 54444559 | — |
| Product | rel-2-Chloro-5-(((3R,5S)-3,5-dimethyl-1-piperidinyl)sulfonyl)benzoic acid | HCID 32335 | — |
Reaction Steps
In the same way, 2-chloro-4-(cis-3,5-dimethylpiperidinosulfonyl)-benzoic acid, m.p. 233°-234° C., is prepared from 2-chloro-4-chlorosulfonylbenzoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04377521 |
| Source dataset | uspto-grants-1983_03 |
| ORD ID | ord-c09cd7d16c784fcfaf3e590a1456e456 |
| Source note | uspto-grants-1983_03 |