Reaction equation
[C:1]([C:3]1[S:4][CH:5]=[CH:6][CH:7]=1)#[N:2].[N+:8]([O-])([OH:10])=[O:9]>C(OC(=O)C)(=O)C>[N+:8]([C:6]1[CH:7]=[C:3]([C:1]#[N:2])[S:4][CH:5]=1)([O-:10])=[O:9]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
To a solution of 2-cyanothiophene (10.9 g; 0.1 mol) in 25 ml of acetic anhydride (t=10° C.) are added 9 ml of fuming nitric acid (d=1.49 g/ml).
Sources & evidence
- ORD record
- ord-4447b93923aa4c0cb9b0badc742f9fbb
- Source dataset
- uspto-grants-1988_08
- Patent number
- US04767758
Linked notes
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