HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sebacic Acid → Bis(tetrabutylammonium)sebacate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sebacic Acid | HCID 5192 | — |
| Reactant | Tetrabutylammonium Hydroxide | HCID 2723671 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Bis(tetrabutylammonium)sebacate | HCID 21903074 | — |
Reaction Steps
The procedure used was the same as described above by titration of sebacic acid (0.814 g, 4.02×10-3 mol) with 1M tetrabutylammonium hydroxide solution in methanol. After removal of solvent, a quantitative yield (2.75 g) of salt was obtained. FIG. 45 shows a 1H NMR spectrum and FIG. 46 shows a 13C NMR spectrum of the salt in CDCl3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05837381 |
| Source dataset | uspto-grants-1998_11 |
| ORD ID | ord-c329fd7522e44baeb9d30c19ddd27df0 |
| Source note | uspto-grants-1998_11 |