Butyl Benzoate → Titanium trichloride butyl benzoate

HRID 358233

Reaction equation

HRID 358233 reaction equation
[Cl-:1].[Cl-].[Cl-].[Ti+3:4].[C:5]([O:13][CH2:14][CH2:15][CH2:16][CH3:17])(=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1>C1(C)C=CC=CC=1>[Cl-:1].[Cl-:1].[Cl-:1].[Ti+3:4].[C:5]([O:13][CH2:14][CH2:15][CH2:16][CH3:17])(=[O:12])[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1

Participants

4

Reactant 2

HCID 8698Butyl BenzoateHCID 10313229titanium(III) trichloride

Product 1

HCID 86739597Titanium trichloride butyl benzoate

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The mixture which was homogenised consisted of 119 g of titanium trichloride, 26 cm3 of butyl benzoate, 390 cm3 of toluene and 3 g of polystyrene ("Lustrex" HF 66). After operating the homogeniser at maximum power for 2.75 minutes, the contents of the flask had formed an immobile gel-like product and the temperature had risen to above 50° C. Homogenisation was terminated and 500 cm3 of toluene were added to assist in the transfer of the dispersed solid to a storage vessel.

Workup

  1. customfor 2.75 minutes
  2. customthe contents of the flask had formed an immobile gel-like product
  3. customhad risen to above 50° C
  4. customHomogenisation was terminated
  5. addition500 cm3 of toluene were added
  6. customto assist in the transfer of the dispersed solid to a storage vessel

Sources & evidence

ORD record
ord-bf204b469be74984850856f66a1f4404
Source dataset
uspto-grants-1984_08
Patent number
US04465783

Linked notes

Loading…