HuagongsheHuagongshe Chemistry Print Report · For research reference only
Anthranilamide → N-[(2-carbamoylphenyl)carbamothioyl]-3-methylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Anthranilamide | HCID 6942 | — |
| Reactant | 3-Methylbenzoyl isothiocyanate | HCID 141397 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | N-[(2-carbamoylphenyl)carbamothioyl]-3-methylbenzamide | HCID 667545 | 89.3% |
Reaction Steps
To a stirred mixture of 7.2 g of 2-aminobenzamide and 200 ml of ether was added dropwise, a solution of 10 g of 3-methylbenzoyl isothiocyanate over 10 minutes. After 48 hours, the solid was collected, giving 14.8 g of the desired product as grey crystals, mp 194°-196° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05001157 |
| Source dataset | uspto-grants-1991_03 |
| ORD ID | ord-0d79b3cbfe21472dbe9de27f6fa957f8 |
| Source note | uspto-grants-1991_03 |