Ethanethioic acid, S-(2-chloro-2-oxoethyl) ester → HCID 178460282, compound

HRID 35970

Reaction equation

HRID 35970 reaction equation
C(S[CH2:5][C:6]([NH:8][C@H:9]1[CH2:14][CH2:13][C@H:12]([O:15][N+:16]([O-:18])=[O:17])[CH2:11][CH2:10]1)=[O:7])(=O)C.O([C@H:23]1CC[C@H](N)CC1)[N+]([O-])=O.C(SCC(Cl)=O)(=O)C>>[C:6]([NH:8][C@H:9]1[CH2:14][CH2:13][C@H:12]([O:15][N+:16]([O-:18])=[O:17])[CH2:11][CH2:10]1)(=[O:7])[CH2:5][CH3:23]

Participants

4

Reactant 3

HCID 82724Ethanethioic acid, S-(2-chloro-2-oxoethyl) esterHCID 178477142HCID 178477142, compoundHCID 178511725HCID 178511725, compound

Product 1

HCID 178460282HCID 178460282, compoundYield 67%

Procedure

2-acetylmercapto-N-(trans-4-nitroxycyclohexyl)acetic acid amide from trans-4-nitroxycyclohexylamine and 2-acetylmercaptoacetic acid chloride melting point: 127°-129° C. (ether), yield: 67% of theory.

Sources & evidence

ORD record
ord-086d97b933f84449a5902622d6ad17f2
Source dataset
uspto-grants-1995_05
Patent number
US05411989

Linked notes

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