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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 36022Generated: October 26, 2026

Acetic Anhydride → HCID 178471962, compound

https://huagongshe.com/reaction/36022

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
ReactantEthyl (3,4,6-Trifluoro-2-methylbenzoyl)acetateHCID 14517129—
Reactant1,2,5-Thiadiazol-3-amine hydrochlorideHCID 19939801—
ReactantEthylorthoformateHCID 53630039—
ProductHCID 178471962HCID 178471962—

Reaction Steps

Compound No. 157 (colorless needles) was prepared in a similar manner to Example 17, proceeding from the corresponding compounds ethyl 2-methyl-3,4,6,-trifluorobenzoylacetate, ethyl orthoformate, acetic anhydride and 3-amino-1,2,5-thiadiazole hydrochloride.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05412098
Source datasetuspto-grants-1995_05
ORD IDord-f2cc6f72bc5242b7979e41784a237d23
Source noteuspto-grants-1995_05