Imidazole → Imidazole isocyanuric acid

HRID 362598

Reaction equation

HRID 362598 reaction equation
[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[C:13](=[O:14])[NH:12][C:10](=[O:11])[NH:9][C:7]1=[O:8]>>[NH:1]1[CH:5]=[CH:4][N:3]=[CH:2]1.[NH:6]1[C:13](=[O:14])[NH:12][C:10](=[O:11])[NH:9][C:7]1=[O:8]

Participants

3

Reactant 2

HCID 795ImidazoleHCID 7956Cyanuric acid

Product 1

HCID 68522078Imidazole isocyanuric acid

Procedure

Heretofore, in a process for obtaining an adduct of imidazole-isocyanuric acid, water, aqueous solution of acetic acid, or dimethylformamide is used as a solvent. An imidazole compound and isocyanuric acid are charged into the solvent as it is in a solid to react by addition, and then crystallized while cooling, thereby being obtained an adduct of imidazole-isocyanuric acid. (confer JP-A-53-116391).

Workup

  1. customto react by addition
  2. customcrystallized
  3. temperaturewhile cooling

Sources & evidence

ORD record
ord-523eaac753074f7b8ebf4e8ee6e19117
Source dataset
uspto-grants-1999_02
Patent number
US05869664

Linked notes

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