Methanesulfonamide → N-[4-(2-bromoethyl)benzoyl]methanesulfonamide

Reaction equation

[CH3:1][S:2]([NH2:5])(=[O:4])=[O:3].[Br:6][CH2:7][CH2:8][C:9]1[CH:17]=[CH:16][C:12]([C:13](Cl)=[O:14])=[CH:11][CH:10]=1>>[Br:6][CH2:7][CH2:8][C:9]1[CH:17]=[CH:16][C:12]([C:13]([NH:5][S:2]([CH3:1])(=[O:4])=[O:3])=[O:14])=[CH:11][CH:10]=1

Participants

Reactant 2

HCID 72879Methanesulfonamide

HCID 140920984-(2-Bromoethyl)benzoyl chloride

Product 1

HCID 67587437N-[4-(2-bromoethyl)benzoyl]methanesulfonamide

Procedure

N-[4-(2-bromoethyl)benzoyl]methanesulfonamide was prepared according to Step 1 of Example 1 from methanesulfonamide and 4-(2-bromoethyl)-benzoyl chloride.

Sources & evidence

ORD record: ord-23bc61e67d134ced9b3b02595965b545
Source dataset: uspto-grants-1999_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05874194

Reaction notes

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