HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Bromophenyl)-1,3-dioxolane → Methyl 2-(1,3-dioxolan-2-yl)-phenylglyoxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Bromophenyl)-1,3-dioxolane | HCID 553534 | — |
| Reactant | Oxalic acid monomethyl ester chloride | HCID 86640482 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | Methyl 2-(1,3-dioxolan-2-yl)-phenylglyoxylate | HCID 21752929 | — |
Reaction Steps
174.5 g of 1-bromo-2-(1,3-dioxolan-2-yl)-benzene was reacted via the zinc-organic compound with 102 g of oxalic acid monomethyl ester chloride, analogously to Example 2. Yield: 41.6 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05416068 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-b55b307c9c064234aa9707ec7ea74f53 |
| Source note | uspto-grants-1995_05 |