HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bas 09531330 → 4H-Pyrido[3,2-e]-1,3-thiazin-4-one, 2-[(4-chlorophenyl)amino]-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bas 09531330 | HCID 973891 | — |
| Reactant | 1-(2-Chloronicotinoyl)-3-(4-chlorophenyl)thiourea | HCID 23287599 | — |
| Product | 4H-Pyrido[3,2-e]-1,3-thiazin-4-one, 2-[(4-chlorophenyl)amino]- | HCID 4292070 | 99.7% |
Reaction Steps
The reaction procedure of (2) of Example 1 was followed except that 6.19 g (19 mmol) of 1-(2-chloronicotinoyl)-3-(4-chlorophenyl)thiourea was used. As a result, 5.49 g of 2-(4-chloroanilino)-4H-pyrido[3,2-e]-1,3-thiazin-4-one was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133258 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-475f0d45dae24f3e86cd31a15cc71f43 |
| Source note | uspto-grants-2000_10 |