HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium thiocyanate → HCID 23287621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium thiocyanate | HCID 15666 | — |
| Reactant | N-methylthiophen-3-amine | HCID 642344 | — |
| Reactant | 2-Chloronicotinoyl chloride | HCID 2774541 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 23287621 | HCID 23287621 | 26.3% |
Reaction Steps
The reaction procedure of Example 102 was followed except that 560 mg of 2-chloronicotinoyl chloride, 242 mg of ammonium thiocyanate, 360 mg of 3-(methylamino)thiophene and 10 ml of acetone were used. The product was then recrystallized from a mixture of ethanol and chloroform to obtain 230 mg of 2-[N-methyl-N-(3-thienyl)amino)-4H-pyrido[3,2-e]-1,3-thiazin-4-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06133258 |
| Source dataset | uspto-grants-2000_10 |
| ORD ID | ord-f44349c4c9634de7b3e5f2bc8b5ad0da |
| Source note | uspto-grants-2000_10 |