HuagongsheHuagongshe Chemistry Print Report · For research reference only
Indole-3-Acetic Acid → HCID 12219383, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Indole-3-Acetic Acid | HCID 802 | — |
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 12219383 | HCID 12219383 | — |
Reaction Steps
To indole-3-acetic acid (186 mg, 1.06 mmol) in 3.5 mL of methylene chloride and 0.009 mL of dimethylformamide, oxalyl chloride (2 M in methylene chloride, 0.64 mL, 1.27 mmol) was added. The mixture was stirred at room temperature for 1 hour and concentrated to give 1H-indole-3-acetyl chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420123 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-b5bb6f04c7054cc0b42ddca249e133b1 |
| Source note | uspto-grants-1995_05 |