Reaction equation
[O-:1][Si:2]([O-:4])=[O:3].[K+:5].[K+].O.[S:8]([O-:12])([OH:11])(=[O:10])=[O:9].[K+].O=O>>[Si:2]([OH:9])([OH:4])([OH:1])[OH:3].[S:8]([O-:12])([O-:11])(=[O:10])=[O:9].[K+:5].[K+:5]Participants
6
Procedure
About equal parts by weight of a dry potassium metasilicate, containing less than 6 mols of water per mol of potassium metasilicate, and potassium hydrogen sulfate are mixed. The mixture is agitated at ambient pressure, and the chemical reaction causes oxygen to evolve in 1 to 3 minutes; considerable heat is produced, and the chemical reaction is complete in 1 to 2 hours, thereby producing white granules of a silicic acid compound and potassium sulfate. The mixture is washed with water and filtered to remove the salt. The silicic acid compound is air dried at 25° to 75° C.
Workup
- additionare mixed
- customthe chemical reaction
- temperatureconsiderable heat
- customis produced
- customthe chemical reaction
- waitis complete in 1 to 2 hours
Sources & evidence
- ORD record
- ord-35a535b328fe47c8a1c25728b821a92e
- Source dataset
- uspto-grants-1978_05
- Patent number
- US04089883
Linked notes
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