Methylcarbamyl fluoride → N-methyl-N-(4-chlorophenylthiosulfenyl)carbamoyl fluoride

Reaction equation

[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([S:8][S:9]Cl)=[CH:4][CH:3]=1.[CH3:11][NH:12][C:13]([F:15])=[O:14]>>[CH3:11][N:12]([S:9][S:8][C:5]1[CH:6]=[CH:7][C:2]([Cl:1])=[CH:3][CH:4]=1)[C:13]([F:15])=[O:14]

Participants

Reactant 2

HCID 12545956Methylcarbamyl fluoride

HCID 134417494-Chlorophenylthiosulfenyl chloride

Product 1

HCID 23333002N-methyl-N-(4-chlorophenylthiosulfenyl)carbamoyl fluoride

Procedure

Prepared by the procedure of Example II by reacting 4-chlorophenylthiosulfenyl chloride with methylcarbamoyl fluoride. b.p. 110°-113° C/0.3 Torr ND24 1.5959.

Workup

customPrepared by the procedure of Example II

Sources & evidence

ORD record: ord-5190e15b808e43d98e4be39d36ec4870
Source dataset: uspto-grants-1978_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04091016

Reaction notes

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