Methyl nadic anhydride → Epoxy-styrene
Reaction equation
C[C:2]12[CH:8]3[C:9]([O:11][C:12](=O)[CH:7]3[CH:4]([CH:5]=[CH:6]1)C2)=O>CC(OOC(=O)C1C=CC=CC=1)(CCC(C)(OOC(=O)C1C=CC=CC=1)C)C>[O:11]1[C:12]([C:7]2[CH:4]=[CH:5][CH:6]=[CH:2][CH:8]=2)=[CH:9]1Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
To this inhibited epoxy diester-styrene mixture about 5.49 parts of NADIC methyl anhydride and about 0.048 part of 2,5-dimethyl-2,5 bis(benzoyl peroxy) hexane catalyst (sold by Wallace & Tiernan Inc. under the Tradename of Luperox 118) were added, as a final step, at 25° C, to provide the solventless epoxy-styrene impregnating resin. The viscosity of the epoxy-styrene impregnating resin was measured to be about 200 cps at 25° C.
Workup
- additionunder the Tradename of Luperox 118) were added
Sources & evidence
- ORD record
- ord-41cbeda50ea7418dae21ca6ef8f49e53
- Source dataset
- uspto-grants-1978_05
- Patent number
- US04091139
Reaction notes
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