Acetic Anhydride → 1-Chloro-4-acetoxy-8-methylnonane
Reaction equation
[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([OH:12])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:11])[CH3:10].[C:13](OC(=O)C)(=[O:15])[CH3:14]>>[Cl:1][CH2:2][CH2:3][CH2:4][CH:5]([O:12][C:13](=[O:15])[CH3:14])[CH2:6][CH2:7][CH2:8][CH:9]([CH3:10])[CH3:11]Participants
3
Procedure
A mixture of 1-chloro-8-methyl-4-nonanol (22.73 g.; 0.118 mole) and acetic anhydride (24.07 g.; 0.236 mole) is heated on a steam bath for 11/2 hours.
Workup
- temperatureis heated on a steam bath for 11/2 hours
Sources & evidence
- ORD record
- ord-6134ef65b1db49c3a3687df6418611f1
- Source dataset
- uspto-grants-1978_05
- Patent number
- US04092356
Reaction notes
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