HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylaniline → 2,2'-Dithiobis[N-(2-ethylphenyl)benzamide]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylaniline | HCID 11357 | — |
| Reactant | 2,2'-Dithiodibenzoyl chloride | HCID 88164 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2,2'-Dithiobis[N-(2-ethylphenyl)benzamide] | HCID 18935325 | 33.6% |
Reaction Steps
This compound was prepared according to the general method of Example 90 using 2,2'-dithiobisbenzoyl chloride (2.00 g, 5.83 mmol) in 50 mL of dichloromethane and 2-ethylaniline (1.40 g, 11.6 mmol) in 12 mL of pyridine. The crude product was recrystallized from acetonitrile-DMF to yield 1.0 g of the title compound, mp 255°-256° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05734081 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-7d989fed42294e84a3366f42f847f891 |
| Source note | uspto-grants-1998_03 |