Reaction equation
[CH:1](=[O:5])[CH2:2][CH2:3][CH3:4]>C(C1OCC(C)(C)CO1)=O>[CH2:3]([C:2](=[CH:1][CH2:2][CH2:3][CH3:4])[CH:1]=[O:5])[CH3:4]Participants
3
Reactant 1
Product 1
Reagents, catalysts & solvents 1
Procedure
A solution of 288 g of n-butyraldehyde in 288 g of 2-formyl-5,5-dimethyl-1,3-dioxane is reacted as described in Example 3, and 285.6 g (72.1% of theory) of 4-neopentylglycol acetal of 2-ethylfumardialdehyde of boiling point 82°-84° C./1 mbar are obtained by fractional distillation, in addition to 128 g of 2-ethylhexenal as light ends.
Sources & evidence
- ORD record
- ord-cddba1c202c4486db1c040563b2f4bcc
- Source dataset
- uspto-grants-1992_11
- Patent number
- US05162552
Linked notes
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