HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenylpiperazine → alpha-{[1-(4-Phenylpiperazinyl)]methyl}benzeneacetic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenylpiperazine | HCID 7096 | — |
| Reactant | Atropic acid | HCID 68114 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | alpha-{[1-(4-Phenylpiperazinyl)]methyl}benzeneacetic acid | HCID 19433570 | — |
Reaction Steps
1-Phenylpiperazine and atropic acid in ethanol is heated under reflux for 18 h, cooled to room temperature, and evaporated in vacuo. The solid is triturated with acetone to give the title product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05420278 |
| Source dataset | uspto-grants-1995_05 |
| ORD ID | ord-ddfe5d50e0a74f92b0510bc2dfbdf66c |
| Source note | uspto-grants-1995_05 |