3'-Aminoacetophenone → N,N'-bis(3-acetylphenyl)pentanediamide

HRID 377032

Reaction equation

HRID 377032 reaction equation
[CH3:1][C:2]([C:4]1[CH:9]=[CH:8][CH:7]=[C:6]([NH2:10])[CH:5]=1)=[O:3].[C:11](Cl)(=[O:18])[CH2:12][CH2:13][CH2:14][C:15](Cl)=[O:16]>>[C:2]([C:4]1[CH:5]=[C:6]([NH:10][C:11](=[O:18])[CH2:12][CH2:13][CH2:14][C:15]([NH:10][C:6]2[CH:7]=[CH:8][CH:9]=[C:4]([C:2](=[O:3])[CH3:1])[CH:5]=2)=[O:16])[CH:7]=[CH:8][CH:9]=1)(=[O:3])[CH3:1]

Participants

3

Reactant 2

HCID 74173'-AminoacetophenoneHCID 17887Pentanedioyl dichloride

Product 1

HCID 1010291N,N'-bis(3-acetylphenyl)pentanediamide

Procedure

N,N'-bis(3,5-diacetylphenyl)(isophthalic acid diamide), mp 283-4° C. Also analogously, N,N'-bis(3-acetylphenyl)pentanediamide, mp 174-5° C. was prepared from 3-aminoacetophenone and glutaryl dichloride.

Sources & evidence

ORD record
ord-6b7cafded22f44a094fa3a0bcef386ed
Source dataset
uspto-grants-2000_02
Patent number
US06022900

Linked notes

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