Ammonia → 5-Imino-1,3,3-trimethylcyclohexane-1-carbonitrile

HRID 377064

Reaction equation

HRID 377064 reaction equation
[C:1]([C:3]1([CH3:12])[CH2:8][C:7]([CH3:10])([CH3:9])[CH2:6][C:5](=O)[CH2:4]1)#[N:2].[NH3:13]>>[C:1]([C:3]1([CH3:12])[CH2:8][C:7]([CH3:10])([CH3:9])[CH2:6][C:5](=[NH:13])[CH2:4]1)#[N:2]

Participants

3

Reactant 2

HCID 222AmmoniaHCID 990683-Cyano-3,5,5-trimethylcyclohexanone

Product 1

HCID 117449815-Imino-1,3,3-trimethylcyclohexane-1-carbonitrile

Procedure

imination of 3-cyano-3,5,5-trimethylcyclohexanone with ammonia in the presence of an imination catalyst at temperatures ranging from 20° to 150° C. and pressures ranging from 1.5 to 30 MPa to form 3-cyano-3,5,5-trimethylcyclohexanone imine followed by

Workup

  1. customranging from 20° to 150° C.

Sources & evidence

ORD record
ord-f80d41fcd0904d42aa5bc29dde0426c6
Source dataset
uspto-grants-2000_02
Patent number
US06022999

Linked notes

Loading…