Ethylamine → HCID 690464, compound

Reaction equation

[Cl:1][C:2]1[CH:10]=[CH:9][C:8]([Cl:11])=[CH:7][C:3]=1[C:4](Cl)=[O:5].[CH2:12]([NH2:14])[CH3:13]>>[CH2:12]([NH:14][C:4](=[O:5])[C:3]1[CH:7]=[C:8]([Cl:11])[CH:9]=[CH:10][C:2]=1[Cl:1])[CH3:13]

Participants

Reactant 2

HCID 6341Ethylamine

HCID 179452,5-Dichlorobenzoyl chloride

Product 1

HCID 690464HCID 690464, compoundYield 85%

Procedure

2,5-Dichlorobenzoyl chloride (51 mmol) and 70% aq EtNH2 (130 mmol) were combined according to General Method El to afford 9.4 g of N-ethyl-2,5-dichloro-benzamide as a beige solid, an 85% yield.

Sources & evidence

ORD record: ord-165b975393444542a2c0f36409dae977
Source dataset: uspto-grants-2000_02
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06028101

Reaction notes

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