Hydrazine hydrate (1:1) → 2-Hydrazinoquinoxaline

Participants

Reaction Conditions

Reaction Steps

15.0 g (91.1 mmol) of 2-chloroquinoxaline are initially charged in 150 ml of ethanol. 45.6 g (911.3 mmol) of hydrazine hydrate are added, and the mixture is stirred under reflux for 16 h. The mixture is then cooled to 0° C., and the solid formed is filtered off, washed with ethanol and dried under high vacuum.

Provenance & Evidence